Sachin Tendulkar fell just six runs short of his 100th international century before tailender Ravichandran Ashwin completed a maiden hundred in the third Test against the West Indies on Friday.
With bat dominating ball throughout the match to make a draw the only likely result, day four was set up for Tendulkar's landmark innings. However, he was dismissed by Ravi Rampaul for 94 to the dismay of a packed crowd in his native Mumbai.
Number eight Ashwin, who had scored just four runs in two innings in his first two matches, soon lifted the mood with an entertaining 103 in 118 balls before he was last man out with the score on 482.
Spinner Pragyan Ojha took two wickets with the new ball as the West Indies began their second innings, which progressed to 81-2 by stumps - a lead of 189.
An expectant crowd packed the Wankhede Stadium in the morning, with the stage seemingly set for Tendulkar to finally reach the unprecedented milestone.
But the 38-year-old's adoring fans were left in stunned silence when, after racing to 94, he edged Rampaul to Darren Sammy at second slip.
Tendulkar had begun the day on 67 and while he took six from the first over, he lost his overnight partner VVS Laxman in the next.
Fidel Edwards removed Laxman (32) with his first ball of the day, slicing a loose drive to Marlon Samuels at gully.
The focus of attention remained very much on Tendulkar though, and he looked set to oblige the waiting Indian public when he upper-cut Edwards for six to coast into the 90s.
At that point Tendulkar had taken 26 runs from 18 balls but with the script nearly complete, he tried to force a back-foot drive off Rampaul that instead flew into the waiting hands of Sammy.
Rampaul then squeezed a yorker into Mahendra Singh Dhoni's stumps as a now-rattled India found themselves in danger of failing to avoid the follow-on at 331-6.
Virat Kohli steadied matters alongside Ashwin in a productive period before lunch.
Kohli registered a maiden Test half-century but fell soon after for 52 to give Devendra Bishoo his first wicket of the match.
Ashwin was slapping the ball to the boundary at will at the other end - including two sixes off Bishoo - but lost both Ishant Sharma (five) and Varun Aaron (four) as he closed in on three figures.
Ojha kept him company as a top-edged four brought him to 99 and a delicate steer through third man ushered in the hundred.
Rampaul beat him for pace off the very next ball to end the innings and bring about tea.
Dhoni threw slow left-armer Ojha the new ball instead of Aaron and was rewarded when he claimed the wicket of Adrian Barath for just three runs.
Kirk Edwards followed for 17 when Dhoni stumped him dancing down the track but Kraigg Brathwaite (34no) and first-innings centurion Darren Bravo (27no) stayed put until stumps.