Leeds' move for Bayern Munich midfielder Michael Cuisance is off after the player failed a medical on Thursday.
The France U20 international had been in Leeds to finalise a deal to become the club's eighth signing of the window.
Cuisance joined Bayern from Borussia Monchengladbach in August 2019 but has made just 11 appearances for the German and European champions.
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He was left out of the squad for Sunday's 4-1 defeat to Hoffenheim and was an unused substitute for the European Super Cup victory over Sevilla, but did play for 17 minutes in Bayern's 8-0 thrashing of Schalke in their opening Bundesliga game.
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Following their return to the Premier League, Leeds have signed Valencia forward Rodrigo Moreno, Real Sociedad defender Diego Llorente, Freiburg defender Robin Koch, Lorient goalkeeper Illan Meslier and Wigan forward Joe Gelhardt.
They have also added Helder Costa from Wolves on a permanent deal following his loan spell last year, and re-signed Jack Harrison on another loan deal from Manchester City.
Transfer Deadline Day - October 5
The summer transfer window closes at 11pm on Monday October 5 with a feast of activity throughout the day involving the biggest names in football.
Some of the highlights to enjoy on Sky Sports News and across our Sky Sportsplatforms:
- Breakfast with David Ginola and Rachel Yankey
- The Football Show Special with Dwight Yorke and Andy Cole
- Countdown with Harry and Jamie Redknapp
- Supporters at the heart of the show with Sky VIP fan wall
You can also follow the stories on Sky Sports' digital platforms, with our dedicated Transfer Centre blog.
Here's all you need to know about Deadline Dayand how to keep across all the deals and drama with Sky Sports.